Problems of Forensic Sciences 1997 Vol. 36 (XXXVI) 132-144
CHROMATOGRAPHIC DETERMINATION OF CARBON MONOXIDE AND CARBOXYHEMOGLOBIN BY THE HEAD-SPACE TECHNIQUE USING A CATALYTIC MICROREACTOR WITH FID DETECTOR
Grzegorz BUSZEWICZ, Roman MĄDRO
Chair and Department of Forensic Medicine, Medical Academy, Lublin
Streszczenie
The following devices were used to determine CO in biological material: a FISONS 8160 gas chromatograph, an FID detector equipped with a nickel microcatalyst and J&W GS-Molesieve column, and also a HS-800 head-space autosampler. This method does not require the addition of any hydrogen admixture to the carrier gas, and is fast and simple. Calibration was successfully used to determine COHb - calibrators were created by saturating blood samples with carbon monoxide.
Słowa kluczowe
Carbon monoxide; Head-space; Catalytic microreactor.